Research Article | Open Access | Download PDF
Volume 13 | Issue 5 | Year 2026 | Article Id. IJME-V13I5P101 | DOI : https://doi.org/10.14445/23488360/IJME-V13I5P101Influence of Duplex Plasma Nitriding and PVD Hard Coatings on the Mechanical and Tribological Performance of Tool Steel
Kolse Chandrashekhar Ashok, R. A. Kapgate
| Received | Revised | Accepted | Published |
|---|---|---|---|
| 01 Feb 2026 | 08 Mar 2026 | 10 Apr 2026 | 29 May 2026 |
Citation :
Kolse Chandrashekhar Ashok, R. A. Kapgate, "Influence of Duplex Plasma Nitriding and PVD Hard Coatings on the Mechanical and Tribological Performance of Tool Steel," International Journal of Mechanical Engineering, vol. 13, no. 5, pp. 1-8, 2026. Crossref, https://doi.org/10.14445/23488360/IJME-V13I5P101
Abstract
Improving the durability of tooling and formation components remains one of their biggest issues. This is due to the severe wear, friction, and deterioration of the surfaces when exposed to high-concentration stresses. Another example of a commonly used surface engineering method is Physical Vapour Deposition (PVD) coating and thermochemical treatment. The techniques are effective in enhancing the general effectiveness of the tool. The overall impact of plasma nitriding and PVD hard coating on tool steel was systematically studied in the current research. It was dedicated to the mechanical and tribological behaviour of the materials. TiCN and TiAlN were coated in order to enhance the surface hardness and wear resistance, following the production of a hardened diffusion layer through plasma nitriding, which was able to bear external loading. Mechanical characterization was also done using microhardness measurement and tribological performance by the use of a dry sliding wear test. The worn surfaces and the coating integrity were analysed by means of X-Ray Diffraction (XRD), Energy-Dispersive Spectroscopy (EDS), and Scanning Electron Microscopy (SEM). The observation demonstrates that the surface hardness of the duplex-treated samples and the singly treated samples significantly differ in their wear rates and surface hardness. The result of the work develops a mechanistic base for higher hybrid surface treatment strategies. Moreover, they offer a reference framework for further optimization and experimental modeling of the engineering tools of surface forming.
Keywords
Nitriding of plasma, PVD hardened coating, TiAlN and TiCN coating, Tribological behaviour.
References
- Tomasz Trzepieciński, “Approaches for Preventing Tool Wear in Sheet Metal Forming Processes,” Machines, vol. 11, no. 6, pp. 1-30, 2023.
[CrossRef] [Google Scholar] [Publisher Link] - S. Pratheesh Kumar et al., “Real-Time Applications and Novel Manufacturing Strategies of Incremental Forming: An Industrial Perspective,” Materials Today: Proceedings, vol. 46, pp. 8153-8164, 2021.
[CrossRef] [Google Scholar] [Publisher Link] - Maziar Ramezani et al., “Surface Engineering of Metals: Techniques, Characterizations and Applications,” Metals, vol. 13, no. 7, pp. 1-31, 2023.
[CrossRef] [Google Scholar] [Publisher Link] - H.S. Aljibori, A. Alamiery, and A.A.H. Kadhum, “Advances in Corrosion Protection Coatings: A Comprehensive Review,” International Journal of Corrosion and Scale Inhibition, vol. 12, no. 4, pp. 1476-1520, 2023.
[CrossRef] [Google Scholar] [Publisher Link] - M. Pellizzari, and A. Molinari, “The Application-Oriented Heat Treatment of Tool Steels,” Materials and Manufacturing Processes, vol. 24, no. 7-8, pp. 723-728, 2009.
[CrossRef] [Google Scholar] [Publisher Link] - Zhou Zhen-yu et al., “Research on the Construction of Gradient Nanostructure and Anti-Tribocorrosion Behavior of Aluminum Alloy Surface,” Tribology International, vol. 194, 2024.
[CrossRef] [Google Scholar] [Publisher Link] - Tasfia Saba et al., “Precise Surface Engineering: Leveraging Chemical Vapor Deposition for Enhanced Biocompatibility and Durability in Biomedical Implants,” Heliyon, vol. 10, no. 18, pp. 1-25, 2024.
[CrossRef] [Google Scholar] [Publisher Link] - D. Dinesh Kumar et al., “Wear Resistant Super-Hard Multilayer Transition Metal-Nitride Coatings,” Surfaces and Interfaces, vol. 7, pp. 74-82, 2017.
[CrossRef] [Google Scholar] [Publisher Link] - Anushiya Manickam et al., “Corrosion Mitigation Strategies for 316 L Stainless Steel in Biomedical Implants: Advances in Materials and Surface Modifications,” Journal of Bio- and Tribo-Corrosion, vol. 12, no. 1, 2026.
[CrossRef] [Google Scholar] [Publisher Link] - Dinesh Kumar Devarajan et al., “State-of-the-Art Developments in Advanced Hard Ceramic Coatings Using PVD Techniques for High-Temperature Tribological Applications,” Ceramics, vol. 6, no. 1, pp. 301-329, 2023.
[CrossRef] [Google Scholar] [Publisher Link] - Sarthak Prasad Sahoo, and Saurav Datta, “Comparative Experimental Study on Application Feasibiility of MTCVD Ticn-Al2O3-Tiocn Multi-Layer Coated Carbide and PVD Tin Single Layer Coated Composite Ceramic Inserts During Dry Machining of Ti-6Al-4V,” Sādhanā, vol. 47, no. 2, 2022.
[CrossRef] [Google Scholar] [Publisher Link] - Harish C. Barshilia, “Surface Modification Technologies for Aerospace and Engineering Applications: Current Trends, Challenges and Future Prospects,” Transactions of the Indian National Academy of Engineering, vol. 6, no. 2, pp. 173-188, 2021.
[CrossRef] [Google Scholar] [Publisher Link] - Yinxia Zhang et al., “Toughening Nitride Hard Coatings by Deflecting Cracks Along Grain Boundaries,” Materials Science and Engineering: A, vol. 935, pp. 1-7, 2025.
[CrossRef] [Google Scholar] [Publisher Link] - Rumana Akhter et al., “Enhancing the Adhesion Strength and Wear Resistance of Nanostructured NiCrN Coatings,” Applied Surface Science, vol. 541, 2021.
[CrossRef] [Google Scholar] [Publisher Link] - Kelsey Ann Vella et al., “The Effect of a Duplex Surface Treatment on the Corrosion and Tribocorrosion Characteristics of Additively Manufactured Ti-6Al-4V,” Materials, vol. 16, no. 5, pp. 1-23, 2023.
[CrossRef] [Google Scholar] [Publisher Link] - Francesca Borgioli, “The Corrosion Behavior in Different Environments of Austenitic Stainless Steels Subjected to Thermochemical Surface Treatments at Low Temperatures: An Overview,” Metals, vol. 13, no. 4, pp. 1-33, 2023.
[CrossRef] [Google Scholar] [Publisher Link] - K. Nikolov et al., “Strip Hollow Cathode Method for Plasma Thermochemical Treatment for Surface Modification of Thin Metal Strips: Plasma Nitriding of Austenitic Stainless Steel Sheets for Bipolar Plates,” Vacuum, vol. 102, pp. 31-37, 2014.
[CrossRef] [Google Scholar] [Publisher Link] - Andresa Baptista et al., “Sputtering Physical Vapour Deposition (PVD) Coatings: A Critical Review on Process Improvement and Market Trend Demands,” Coatings, vol. 8, no. 11, pp. 1-22, 2018.
[CrossRef] [Google Scholar] [Publisher Link] - J. Zheng et al., “Microstructures and Mechanical Properties of Duplex-Treated Composite Ceramic Coatings with and Without Compound Layer,” Ceramics International, vol. 41, no. 2, pp. 2519-2526, 2015.
[CrossRef] [Google Scholar] [Publisher Link] - A.A. Vereschaka et al., “Delamination and Longitudinal Cracking in Multi-Layered Composite Nano-Structured Coatings and their Influence on Cutting Tool Life,” Wear, vol. 390-391, pp. 209-219, 2017.
[CrossRef] [Google Scholar] [Publisher Link] - M.A. Al-Bukhaiti et al., “Tribological and Mechanical Properties of Ti/TiAlN/TiAlCN Nanoscale Multilayer PVD Coatings Deposited on AISI H11 Hot Work Tool Steel,” Applied Surface Science, vol. 318, pp. 180-190, 2014.
[CrossRef] [Google Scholar] [Publisher Link] - M. Roseen, “Influence of Pulsing on PVD Tialn Coating Microstructure and Mechanical Properties: Master Thesis Project on the Impact of Deposition Parameters on Performance and Properties of PVD Titanium Aluminum Nitride,” 2023.
[Google Scholar] - Monika Madej, and Katarzyna Piotrowska, “Characterisation of TiCN Coatings for Biomedical Applications,” Coatings, vol. 14, no. 6, pp. 1-13, 2024.
[CrossRef] [Google Scholar] [Publisher Link] - Şengül Danışman, Durmuş Odabaş, and Muharrem Teber, “The Effect of TiN, TiAlN, TiCN Thin Films Obtained by Reactive Magnetron Sputtering Method on the Wear Behavior of Ti6Al4V Alloy: A Comparative Study,” Coatings, vol. 12, no. 9, pp. 1-19, 2022.
[CrossRef] [Google Scholar] [Publisher Link] - Jinju Chen, and S.J. Bull, “Approaches to Investigate Delamination and Interfacial Toughness in Coated Systems: An Overview,” Journal of Physics D: Applied Physics, vol. 44, no. 3, 2010.
[CrossRef] [Google Scholar] [Publisher Link] - Di Wang et al., “Microstructure Effects on Fracture Failure Mechanism of CrAl/CrAlN Coating,” Ceramics International, vol. 47, no. 3, pp. 3657-3664, 2021.
[CrossRef] [Google Scholar] [Publisher Link] - Wenzheng Zhai et al., “Recent Progress on Wear‐Resistant Materials: Designs, Properties, and Applications,” Advanced Science, vol. 8, no. 11, pp. 1-29, 2021.
[CrossRef] [Google Scholar] [Publisher Link]